Brookfield DV-III Ultra Rheometer Manual de usuario Pagina 1

Brookeld Engineering Laboratories, Inc. Page 1 Manual No. M98-211-E0912BROOKFIELD DV-III ULTRAProgrammable RheometerOperating InstructionsMan

Brookeld Engineering Laboratories, Inc. Page 10 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 10 Manual No.

Brookeld Engineering Laboratories, Inc. Page 100 Manual No. M98-211-E0912 Universal Spindle Ranges (cont.)Spindle Entry CodeSPINDLE RANGE CO

Brookeld Engineering Laboratories, Inc. Page 101 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 101 Manual No

Brookeld Engineering Laboratories, Inc. Page 102 Manual No. M98-211-E0912 ThermoselSpindleShear Rate (sec-1)Viscosity (cP)LVDV-III Ultra RVD

Brookeld Engineering Laboratories, Inc. Page 103 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 103 Manual No

Brookeld Engineering Laboratories, Inc. Page 104 Manual No. M98-211-E0912In taking viscosity measurements with the DV-III Ultra Rheometer the

Brookeld Engineering Laboratories, Inc. Page 105 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 105 Manual No

Brookeld Engineering Laboratories, Inc. Page 106 Manual No. M98-211-E0912A repeatable viscosity test should control or specify the following:

Brookeld Engineering Laboratories, Inc. Page 107 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 107 Manual No

Brookeld Engineering Laboratories, Inc. Page 108 Manual No. M98-211-E0912Table D-1 (continued)SPINDLE ENTRY CODE SMC SRCT-D 94 200 0T-E 95

Brookeld Engineering Laboratories, Inc. Page 109 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 109 Manual No

Brookeld Engineering Laboratories, Inc. Page 11 Manual No. M98-211-E0912 I.8 Safety Symbols and Precautions Safety Symbols The followi

Brookeld Engineering Laboratories, Inc. Page 110 Manual No. M98-211-E0912 Two constants are required: a) SMC (Spindle Multiplier Constan

Brookeld Engineering Laboratories, Inc. Page 111 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 111 Manual No

Brookeld Engineering Laboratories, Inc. Page 112 Manual No. M98-211-E0912The shear stress measurement range for the three standard (or suppli

Brookeld Engineering Laboratories, Inc. Page 113 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 113 Manual No

Brookeld Engineering Laboratories, Inc. Page 114 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 114 Manual No

Brookeld Engineering Laboratories, Inc. Page 115 Manual No. M98-211-E0912Table E-1 Normal 25°C Standard Fluids High Temperature Standard F

Brookeld Engineering Laboratories, Inc. Page 116 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 116 Manual No

Brookeld Engineering Laboratories, Inc. Page 117 Manual No. M98-211-E09125) Measure the viscosity and record the Rheometer reading.Note: Th

Brookeld Engineering Laboratories, Inc. Page 118 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 118 Manual No

Brookeld Engineering Laboratories, Inc. Page 119 Manual No. M98-211-E09125) Connect the sample cup to the Rheometer. Allow sufcien

Brookeld Engineering Laboratories, Inc. Page 12 Manual No. M98-211-E09121) Place the upright rod into the hole at the front of the base. The

Brookeld Engineering Laboratories, Inc. Page 120 Manual No. M98-211-E0912 APPENDIX F - The Brookeld GuardlegThe guard leg was originally des

Brookeld Engineering Laboratories, Inc. Page 121 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 121 Manual No

Brookeld Engineering Laboratories, Inc. Page 122 Manual No. M98-211-E0912 APPENDIX G - DV-III Ultra Stand AssemblyDV-III Ultra Stand Assembly

Brookeld Engineering Laboratories, Inc. Page 123 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 123 Manual No

Brookeld Engineering Laboratories, Inc. Page 124 Manual No. M98-211-E0912 APPENDIX I - DV-III Ultra to Computer Command SetSerial (RS-232) Co

Brookeld Engineering Laboratories, Inc. Page 125 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 125 Manual No

Brookeld Engineering Laboratories, Inc. Page 126 Manual No. M98-211-E0912xx = The rmware version of the instrument (i.e. version 4.1 is re

Brookeld Engineering Laboratories, Inc. Page 127 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 127 Manual No

Brookeld Engineering Laboratories, Inc. Page 128 Manual No. M98-211-E0912 APPENDIX J - Fault Diagnosis and TroubleshootingListed are some of

Brookeld Engineering Laboratories, Inc. Page 129 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 129 Manual No

Brookeld Engineering Laboratories, Inc. Page 13 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 13 Manual No.

Brookeld Engineering Laboratories, Inc. Page 130 Manual No. M98-211-E0912 ❑ Rheometer Will Not Communicate With PC✓ Check the comm port set

Brookeld Engineering Laboratories, Inc. Page 131 Manual No. M98-211-E0912 APPENDIX K - Online Help and Additional Resourceswww.brookeldengin

Brookeld Engineering Laboratories, Inc. Page 132 Manual No. M98-211-E0912 APPENDIX L - Warranty Repair and ServiceWarrantyBrookeld Viscomete

Brookeld Engineering Laboratories, Inc. Page 133 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 133 Manual No

Brookeld Engineering Laboratories, Inc. Page 14 Manual No. M98-211-E0912ANAL OG OUTPUT STORQUE 0-1V TEMP 10MV/ CoMODEL DV-III ULTRA

Brookeld Engineering Laboratories, Inc. Page 15 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 15 Manual No.

Brookeld Engineering Laboratories, Inc. Page 16 Manual No. M98-211-E0912 S STRIP CHART RECORDER DVP-96Y cable is used to connect the serial

Brookeld Engineering Laboratories, Inc. Page 17 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 17 Manual No.

Brookeld Engineering Laboratories, Inc. Page 18 Manual No. M98-211-E0912 II. GETTING STARTED II.1 AutozeroBefore readings may be taken, t

Brookeld Engineering Laboratories, Inc. Page 19 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 19 Manual No.

Brookeld Engineering Laboratories, Inc. Page 2 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 2 Manual No. M9

Brookeld Engineering Laboratories, Inc. Page 20 Manual No. M98-211-E0912ITEM PRINT FORMAT RANGE EXAMPLERPM RPMX.XXXX.XXXX.X 0.01 <= RPM

Brookeld Engineering Laboratories, Inc. Page 21 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 21 Manual No.

Brookeld Engineering Laboratories, Inc. Page 22 Manual No. M98-211-E0912VISCOMETER SETUPPRESS ENTER TO STARTFigure II-9Press the ENTER key.

Brookeld Engineering Laboratories, Inc. Page 23 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 23 Manual No.

Brookeld Engineering Laboratories, Inc. Page 24 Manual No. M98-211-E0912and the display will be updated to the next screen image:RPM: 112 S

Brookeld Engineering Laboratories, Inc. Page 25 Manual No. M98-211-E0912 II.6 Preventative Maintenance The DV-III Ultra does not require

Brookeld Engineering Laboratories, Inc. Page 26 Manual No. M98-211-E0912• Wells/Brookeld sample cups should be handled carefully to prevent

Brookeld Engineering Laboratories, Inc. Page 27 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 27 Manual No.

Brookeld Engineering Laboratories, Inc. Page 28 Manual No. M98-211-E0912H) Press the ENTER button on the rheometer to run the test. The scr

Brookeld Engineering Laboratories, Inc. Page 29 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 29 Manual No.

Brookeld Engineering Laboratories, Inc. Page 3 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 3 Manual No. M9

Brookeld Engineering Laboratories, Inc. Page 30 Manual No. M98-211-E0912 III.3 Selecting a Spindle/SpeedThe DV-III Ultra has the capabilit

Brookeld Engineering Laboratories, Inc. Page 31 Manual No. M98-211-E0912 IV. PROGRAMMING THE DV-III ULTRA AND DATA COLLECTION M

Brookeld Engineering Laboratories, Inc. Page 32 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 32 Manual No.

Brookeld Engineering Laboratories, Inc. Page 33 Manual No. M98-211-E0912At this point, the user may Enter/Edit, Clear or Use a stored program

Brookeld Engineering Laboratories, Inc. Page 34 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 34 Manual No.

Brookeld Engineering Laboratories, Inc. Page 35 Manual No. M98-211-E0912 The user inputs his step RPM exactly as he did for nite step time

Brookeld Engineering Laboratories, Inc. Page 36 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 36 Manual No.

Brookeld Engineering Laboratories, Inc. Page 37 Manual No. M98-211-E0912 In which the DV-III Ultra is requesting that the user specically p

Brookeld Engineering Laboratories, Inc. Page 38 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 38 Manual No.

Brookeld Engineering Laboratories, Inc. Page 39 Manual No. M98-211-E0912 S USING PROGRAMMED SPEEDS WITH A ZERO TIME INTERVAL Assume the foll

Brookeld Engineering Laboratories, Inc. Page 4 Manual No. M98-211-E0912 IV.7.5 Other Common Rheological Models ...

Brookeld Engineering Laboratories, Inc. Page 40 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 40 Manual No.

Brookeld Engineering Laboratories, Inc. Page 41 Manual No. M98-211-E0912 Had the user selected a subset of a speed set (Figure IV-15), say s

Brookeld Engineering Laboratories, Inc. Page 42 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 42 Manual No.

Brookeld Engineering Laboratories, Inc. Page 43 Manual No. M98-211-E0912• An internal clock that keeps time between each printed data line (

Brookeld Engineering Laboratories, Inc. Page 44 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 44 Manual No.

Brookeld Engineering Laboratories, Inc. Page 45 Manual No. M98-211-E0912 Click the Delete button to delete the command in the selected

Brookeld Engineering Laboratories, Inc. Page 46 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 46 Manual No.

Brookeld Engineering Laboratories, Inc. Page 47 Manual No. M98-211-E0912Command Command Description Parameter CommentsSSP Set spindle 31 set

Brookeld Engineering Laboratories, Inc. Page 48 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 48 Manual No.

Brookeld Engineering Laboratories, Inc. Page 49 Manual No. M98-211-E0912 Programs are run by pressing the “2” key when in Figure IV-32 which

Brookeld Engineering Laboratories, Inc. Page 5 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 5 Manual No. M9

Brookeld Engineering Laboratories, Inc. Page 50 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 50 Manual No.

Brookeld Engineering Laboratories, Inc. Page 51 Manual No. M98-211-E0912ERRORYOU CANNOT EXECUTE A MATH MODEL BECAUSE NO DATA IS IN BUFFERFigu

Brookeld Engineering Laboratories, Inc. Page 52 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 52 Manual No.

Brookeld Engineering Laboratories, Inc. Page 53 Manual No. M98-211-E0912 Plastic Viscosity (cP or mPa•s) Yield Stress (Dynes/cm2 or N/m

Brookeld Engineering Laboratories, Inc. Page 54 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 54 Manual No.

Brookeld Engineering Laboratories, Inc. Page 55 Manual No. M98-211-E0912Figure IV-44: Test ScreenFigure IV-45: Run/Data Screen

Brookeld Engineering Laboratories, Inc. Page 56 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 56 Manual No.

Brookeld Engineering Laboratories, Inc. Page 57 Manual No. M98-211-E0912 IV.7 Math Models IV.7.1 The Power Law (Ostwald) Model

Brookeld Engineering Laboratories, Inc. Page 58 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 58 Manual No.

Brookeld Engineering Laboratories, Inc. Page 59 Manual No. M98-211-E0912 Figure IV-49When should you use it?The Hersche

Brookeld Engineering Laboratories, Inc. Page 6 Manual No. M98-211-E0912 I.3 Yield Stress MeasurementAnother feature now available in the

Brookeld Engineering Laboratories, Inc. Page 60 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 60 Manual No.

Brookeld Engineering Laboratories, Inc. Page 61 Manual No. M98-211-E0912 An Example of the Bingham Model at WorkA manufacturer of drilling 

Brookeld Engineering Laboratories, Inc. Page 62 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 62 Manual No.

Brookeld Engineering Laboratories, Inc. Page 63 Manual No. M98-211-E0912 Figure IV-51When chocolate is used for enrobin

Brookeld Engineering Laboratories, Inc. Page 64 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 64 Manual No.

Brookeld Engineering Laboratories, Inc. Page 65 Manual No. M98-211-E0912 IV.8 Yield Stress Test Programs and Test SamplesThis section expl

Brookeld Engineering Laboratories, Inc. Page 66 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 66 Manual No.

Brookeld Engineering Laboratories, Inc. Page 67 Manual No. M98-211-E0912Pre-shearing is the shearing of sample before measuring its yield pro

Brookeld Engineering Laboratories, Inc. Page 68 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 68 Manual No.

Brookeld Engineering Laboratories, Inc. Page 69 Manual No. M98-211-E0912The Open File dialog box automatically displays les of the type it

Brookeld Engineering Laboratories, Inc. Page 7 Manual No. M98-211-E0912 I.4 Components Component Part NumberDV-III Ultra Rheometer

Brookeld Engineering Laboratories, Inc. Page 70 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 70 Manual No.

Brookeld Engineering Laboratories, Inc. Page 71 Manual No. M98-211-E0912 DownloadSelecting Download (using the Download button or the

Brookeld Engineering Laboratories, Inc. Page 72 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 72 Manual No.

Brookeld Engineering Laboratories, Inc. Page 73 Manual No. M98-211-E0912 Strain This eld displays the Apparent Strain placed on the sample

Brookeld Engineering Laboratories, Inc. Page 74 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 74 Manual No.

Brookeld Engineering Laboratories, Inc. Page 75 Manual No. M98-211-E0912Graphs Page Options ToolbarNote: Many of the Options buttons are two

Brookeld Engineering Laboratories, Inc. Page 76 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 76 Manual No.

Brookeld Engineering Laboratories, Inc. Page 77 Manual No. M98-211-E0912The spindle was immersed to the primary immersion mark and pre-shear

Brookeld Engineering Laboratories, Inc. Page 78 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 78 Manual No.

Brookeld Engineering Laboratories, Inc. Page 79 Manual No. M98-211-E0912Figure IV-65Figure IV-66: Ketchup Comparison Samples

Brookeld Engineering Laboratories, Inc. Page 8 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 8 Manual No. M9

Brookeld Engineering Laboratories, Inc. Page 80 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 80 Manual No.

Brookeld Engineering Laboratories, Inc. Page 81 Manual No. M98-211-E0912Figure IV-68: Stress vs. Strain Graphs for Various Food ProductsIV.8.

Brookeld Engineering Laboratories, Inc. Page 82 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 82 Manual No.

Brookeld Engineering Laboratories, Inc. Page 83 Manual No. M98-211-E0912 #5: Sample Tst S:71 PRE-SHEARING... RPM: 010 TIME: 0030Figure IV

Brookeld Engineering Laboratories, Inc. Page 84 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 84 Manual No.

Brookeld Engineering Laboratories, Inc. Page 85 Manual No. M98-211-E0912IV.8.6.1 Data OutputPre-Test OutputWhen a test is begun, the followi

Brookeld Engineering Laboratories, Inc. Page 86 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 86 Manual No.

Brookeld Engineering Laboratories, Inc. Page 87 Manual No. M98-211-E0912IV.8.6.3 Test ResultsTest PassedWhen a yield test runs successfully,

Brookeld Engineering Laboratories, Inc. Page 88 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 88 Manual No.

Brookeld Engineering Laboratories, Inc. Page 89 Manual No. M98-211-E0912V. OPTIONSThe DV-III+ Options Menu allows the user to execute tempera

Brookeld Engineering Laboratories, Inc. Page 9 Manual No. M98-211-E0912 I.6 Utilities Auto-sensing Power Supply: Input Voltage: 90

Brookeld Engineering Laboratories, Inc. Page 90 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 90 Manual No.

Brookeld Engineering Laboratories, Inc. Page 91 Manual No. M98-211-E0912 5) Press the OPTION/TAB key to move the cursor to the HI ALARM % 

Brookeld Engineering Laboratories, Inc. Page 92 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 92 Manual No.

Brookeld Engineering Laboratories, Inc. Page 93 Manual No. M98-211-E09123) The DV-III Ultra may be set-up to “handshake” (using XOn/XOff pro

Brookeld Engineering Laboratories, Inc. Page 94 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 94 Manual No.

Brookeld Engineering Laboratories, Inc. Page 95 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 95 Manual No.

Brookeld Engineering Laboratories, Inc. Page 96 Manual No. M98-211-E0912 A.2 SET-UP1. Be sure that the Viscometer is securely mounte

Brookeld Engineering Laboratories, Inc. Page 97 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 97 Manual No.

Brookeld Engineering Laboratories, Inc. Page 98 Manual No. M98-211-E0912 A.4 VERIFYING CALIBRATION1. Determine the appropriate sample vol

Brookeld Engineering Laboratories, Inc. Page 99 Manual No. M/98-211-B0104 Brookeld Engineering Laboratories, Inc. Page 99 Manual No.